?H2O. Blog. Hydrates Lab Report Final - Chemistry Exp: Explore And Evaluate Bonding Properties Hydrates Hydrates Lab Report. As 6.63:1 is relatively close to 7:1, the expected ratio for this substance, we can thus conclude that the unknown hydrate is magnesium sulfate heptahydrate, MgSO. CONCLUSION. Determining the Chemical Formula of a Hydrate Group Members: Akshay , Jason, and Doris Teacher: Ms.Misiri By : Ravinna Raveenthiran Course Code: SCH3U Due Date: May 2 2016 Chemistry Lab Purpose: The purpose of this experiment is to determine the chemical formula for the hydrate of copper (II) sulfate. 3. As we altered the strength of the flame from low to high without increasing the amount of time to wait until all the water can evaporate, there could have possibly been some water left in the beaker with magnesium sulfate that did not evaporate to completion. At the end of the lab is an example page of how to do the calculations on page 22 after you have completed the data. They cost $9.00 if you break it. 3. Some sources of deviation of the data may include: a. Anhydrate. ?H2O. The error being only 5.58%, the overall ratio of water to magnesium sulfate was somewhat accurate. Purpose. If the bunsen burner left some black soot on the bottom of your crucible, how would this change your answer? 1. From this data we determined the moles of the hydrate and, the water in the hydrate, then divided each mole by the smallest mole to find the ratio. formula of hydrate. Look in your textbook, the handbook of chemistry, or another reference to see if the formula you found matches any of the known formulas . If we had either heated the beaker with a strong flame from the beginning or increased the amount of time of heating, the number of moles of water during calculation could have been larger. 2) dry hydrate = (mass of sample + container after heating) - (container) 3) grams of water = grams of hydrate - dry hydrate 4) use grams of the dry sample and water and convert moles 5) divide by smallest mol to find empirical formula 6) you now have found how many water molecules are attached in the hydrate. A loss in the amount of hydrate due to some popping out of the beaker while heating. An example would be CaSO4 . You can now find the percent of the anhydrous salt and the water. Why did we place a beaker over the anhydrous salt as it cooled? 3) Determine the mass of the water lost by the hydrate to produce the anhydrous salt. 2) Determine the number of moles of anhydrous salt present in the crucible. an ionic substance that is chemically combined with loosely held water molecules in a definite ratio. Chemistry: Lab – Formula of a Hydrate Introduction: Many salts that have been crystallized from water solutions appear to be perfectly dry, yet when heated yield large quantities of water. However, as we dehydrated the hydrate and discovered that a hydrate is made of some anhydrate and water with a certain ratio, we soon realized what a hydrate actually was. 2. % water in the hydrate 3a. 3.) Copper(II) sulfate pentahydrate is an example of such a hydrate. However, there must be a few sources of errors that affected the data. By multiplying the mass of the anhydrate, which is magnesium sulfate in the experiment, with its molar mass, the number of moles present at the end can be determined. This suggests that water was present as part of the crystal structure. Crucibles are VERY FRAGILE. We could have not gotten rid of the water in the hydrate to begin with as 15 minutes of heating was perhaps too short. Ratio X:Y 3d. Thus, at the end, we learned that there are countless numbers of applications of stoichiometry in chemistry. The crystals change form, and sometimes color, as the water is driven off. The lab work has two objectives: first, confirm the formula of a hydrate with known formula and second, find the formula of a hydrate in which the salt formula is known but not the molar amount of water. of the substance was 4.24 g and after we heated it a few times the ending mass was 3.62 g. Now I have to figure out what I have. The five in front of the formula for water tells us there are 5 water molecules per formula unit of CuSO 4 (or 5 moles of water per mole of CuSO 4). Formula of the hydrate: MgSO4 • 4H2O Other than causing people to go crazy and/or eat people's faces off and being an excellent substance for bath time relaxation, magnesium sulfate is a prime compound for hydration labs. Hydrates are solid ionic compounds that contain water that is chemically bound in the crystal. Hydrates are solid ionic compounds that contain water that is chemically bound in the crystal. When we heated the hydrated salts, the hydrates evaporated and we were able to find the formula of the salts. Show work, include units, and put your answers in the blanks. The exact definition of a hydrate - any substance that contains some amount of water molecules in its structures - was illustrated in a precise way in this experiment. In this lab, we learned how to apply stoichiometry in a new way to determine a formula of a hydrate. Once we know how much water is needed for each magnesium sulfate, we can then name the substance in MgSO. The beginning weight (uh mass?) (Hint: the An example would be CaSO 4. Iron (III) sulfate has a purple tint to it, and has a crystalline structure. CuSO4 x 5H2O (s) -> CuSO4 (s) + 5H2O (g) My chemistry class had a lab where he gave us all different amounts of unknown substances that were hydrates. What is the mass of copper (II) sulfate? These compounds are called hydrates. 1. My lab partner and I measured and did all that good stuff. The number of water moles can also be known by repeating the same procedure, but with the molar mass of water instead. Safety: Crucibles are VERY HOT; always handle them with tongs. represents the ratio. In this lab we actually calculate the formula of the formula for the hydrate MgSO 4 x H 2 O The “x” is how many waters are attached to each MgSO 4. At the end of the lab is an example page of how to do the calculations on page 22 after you have completed the data. 6. Formula of your hydrate Post Lab Questions. You will be using the hydrate CuSO4 . Observing our nitrate, it has a white crystalline structure, representing that similar to table salt. without water. These resources were hosted on the Chemistry for Biologists website, which launched in 2004 and was supported by the Royal Society of Chemistry and the Biochemical Society. The water in the formula is referred to as the water of To determine the formula of a hydrate experimentally, we must calculate the mole: mole ratio of the water portion compared to the anhydrate portion. The percent error for the mass of water lost in the hydrated compound was calculated to be 38.8%. First, the assumption that the hydrate is associated with magnesium sulfate due to its white appearance is proven to be correct. Calculate the theoretical percentage of water in CuSO4 ( 5 H2O . 2.) Why is it important to heat the baking dish or ramekin and cover in step #1? The water is chemically combined with the salt in a definite ratio. STUDY. Unfamiliar with hydrates, we were first oblivious to how one could experimentally come up with a correct formula. Problem #2: A hydrate of Na 2 CO 3 has a mass of 4.31 g before heating. 1) Determine the mass of the anhydrous salt alone (that is, without the crucible and cover). composition of hydrates lab answers, LAB % COMPOSITION OF A HYDRATE.docx. (40.08 + 32.066 + 4(15.999) + 3(2(1.0079) + 15.999)) = 190.19 g/mol. Print out this page also. After comparing experimentally acquired ratios to the factual ratios for each substance, we determined that the ratios of magnesium sulfate was the closest one out of all four. Record all of the masses until there is no more water left. According to a smaller ratio compared to the expected ratio, more water was probably lost during this occurrence, which lowered the number of water moles. We found that the total mass of the crucible and the hydrate weighed 39.2g before heating and, after heating, it weighed 35.0g, thus there were 3.8g of water in the hydrate. b. 2. Let us look at the big picture... What is a hydrate? Our unknown hydrate may be a hydrate of copper(II) sulfate, magnesium sulfate, iron(III) chloride, or iron(III) nitrate. Chemistry: Lab – % Composition of a Hydrate Introduction: Salt Compounds that contain water molecules attached are called hydrates, or hydrated salts. Digication ePortfolio :: General Chemistry (Alexander Antonopoulos) by Alexander P. Antonopoulos at Salve Regina University. Formula of a Hydrate (Anhydrous Solid ⋅ x H 2 O) The formula of a hydrate can be determined by dehydrating a known mass of the hydrate, then comparing the masses of the original hydrate and the resulting anhydrous solid. The ratios between molecules are in integers, but as this is an experiment, it will be more likely to acquire the ratio in decimal points. The formula of a hydrate … When finding the mass of this chemical, you find the mass of the calcium sulfate and then add 3 times the mass of water to it. The crystals change form, and sometimes color, as the water is driven off. Over 1 million people now use Prezi Video to share content with their audiences For example, the ratio we got from an experiment for iron (III) nitrate was 13.3:1 while it should have been 9:1, according to the information from the resource. How can we experimentally determine the formula of an unknown hydrate, A? The last idea we learned was how to apply the knowledge of colors of specific ions and solids. Iron (III) chloride usually has a bright yellow appearance. Its experimental ratio was 6.63 to 1 and its expected ratio was 7:1. 4. PURPOSE: To determine the percentage of water in a hydrate. Print out this page also. MgSO4 x 1mol = .0083 mol MgSO4 120.4g. This chemical would be called calcium sulfate trihydrate. The ratios of other three substances were incongruous to each other. , we can exclude that option from our prediction. Never carry them around without a heat-proof pad under it. In … The five in front of the formula for water tells us there are 5 water molecules per formula unit of CuSO 4 (or 5 moles of water per mole of CuSO 4). The general formula for mass percent is: (mass of the part you want / mass of the entire sample) x 100% Record your answers above. Zinc sulfate hydrate Trial 1 Trial 2 18.554 21.020 26.768 28.972 Mass of crucible (g) Mass of crucible & sample before heating (g) Mass crucible & sample after heating (g) Mass of hydrate (g) Mass of anhydrous solid (g) 23.165 25.499 Mass of water driven off Moles of water Moles of anhydrous solid Moles of water per mole of zinc sulfate Formula of hydrate You then heat your hydrate until you have a constant weight of 22.04 grams. Complete the folowing and submit your answers as a word document in Canvas. Problem #2: A hydrate of Na 2 CO 3 has a mass of 4.31 g before heating. Hydrate Lab 5. Ratios vary in different hydrates but are specific for any given hydrate. Jan. 26, 2021. A hydrate is a compound that is chemically combined with water molecules. Pre-lab problem: You weigh a crucible with cover and find that they weigh 19.12 grams. The water in the formula is referred to as the water of In this lab we actually calculate the formula of the formula for the hydrate MgSO 4 x H 2 O The “x” is how many waters are attached to each MgSO 4. Testable Prediction: Our unknown hydrate may be a hydrate of copper(II) sulfate, magnesium sulfate, iron(III) chloride, or iron(III) nitrate. This chemical would be called calcium sulfate trihydrate. Introduction: A hydrate is a chemical that has water molecules loosely bonded to it. The water molecules are not actually part of the formula, so the formula is written slightly differently. The number of water molecules in a typical hydrate is characteristic of the particular salt and is usually a small whole number from 1 to 10. By knowing that ions such as Cu, have their designated colors, we were able to eliminate three options for the anhydrate, FeCl. An insufficient amount of time for waiting until all water of the hydrate evaporated. Observing our nitrate, it has a white crystalline structure, representing that similar to table salt. After heating, the mass of the anhydrous compound is found to be 3.22 g. Determine the formula of the hydrate and then write out the name of the hydrate. Magnesium sulfate, the only left option, is white in appearance which makes it a possible identification for our hydrate. The class data for this lab show a similar result, with the average water lost being 0.365g and the percentage by mass of water in the compound being 30.3%. By knowing that ions such as Cu2+ and Fe3+ have their designated colors, we were able to eliminate three options for the anhydrate, FeCl3, Fe(No3)3, and CuSO4, as the hydrate appeared to be white due to the colorless magnesium.Thus, this knowledge of specific colors of ions led us to confidently conclude that the anhydrate was undoubtedly magnesium sulfate. Then, the experimental ratio of water to magnesium sulfate being 6.63 to 1 with about 6% error strongly supports our hypothesis to a deeper level. Moles water 3c. Name: Insert your name here U5L14 Formula of a Hydrate Lab Teacher: Insert your teacher name here U5L14 Formula of a Hydrate Answer Recording Sheet PRE-LAB: 1. Furthermore, this lab illustrated a new term for the group - hydrate. University. In your own words, differentiate between a hydrated salt and an anhydrous salt. Obtain a scoop of the hydrate from your teacher and find the mass again. properties of hydrates lab answers, About Chemistry for Biologists Chemistry for Biologists resources aim to help you understand the chemistry and chemical principles that underlie a good deal of biology. This hydrate was previously mentioned in class to be magnesium sulfate heptahydrate. What is the formula of the hydrate? Engage students in your virtual classroom with Prezi Video for Google Workspace; Jan. 20, 2021. The last idea we learned was how to apply the knowledge of colors of specific ions and solids. Mass of water 2d. Lab – Formula of a Hydrate - Help with calculations Magnesium sulfate ( MgSO 4) is a molecule that loves to hold on to water (hydrophilic). Lab 2: Determine the Percentage of Water in a Hydrate: The goal of this experiment is to learn how to properly calculate the ratio of salt to water, in a hydrated salt, and to calculate the percentage of water (by mass) within a hydrated salt. They are crystalline compounds that have a specific number of water molecules trapped within the crystal lattice. Its formula is CuSO 4 5H 2 O. The crucible, cover and hydrate weigh 22.69 grams. ; As 6.63:1 is relatively close to 7:1, the expected ratio for this substance, we can thus conclude that the unknown hydrate is magnesium sulfate heptahydrate, MgSO4 7H2O. Thus, the ratio between water and magnesium sulfate will be close to being 7:1. Because the number of moles of water was lower than what it could have been originally, the ratio of water to anhydrate was 6:63:1 rather than 7:1. c. Change in the strength of the heat while maintaining the same amount of time to heat. Show all calculations in the calculations section. At the end of the lab is an example page of how to do the calculations on page 22 after you have completed the data. Place an inverted beaker over it while cooling. 3.) PLAY. Find the mass of a clean, dry crucible. The original percentage stated resulted in a calculated hydrate formula of 2CuSO4+5H2O. The actual hydrate formula for the copper (II) sulfate compound was CuSO4+5H2O. Furthermore, in order to determine the exact name of the hydrate, we must find out the ratio between the anhydrate and water that are associated with the hydrate. Let the crucible cool and find its mass again. You will be weighing a hydrate and heating it to remove the water (now called "anhydrous salt") and weigh it again. Compare your experimental percentage to theoretical percentage for water in the hydrate. Lab – Formula of a Hydrate - Help with calculations Magnesium sulfate ( MgSO 4) is a molecule that loves to hold on to water (hydrophilic). Virtual Lab Hydrate.docx. This phenomenon could have deviated the ratio by causing a loss in the amount of water and anhydrate. Use the information to answer the questions. Hydrate Lab. 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